BMRB Entry 5446
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5446
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Citation: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John. "NMR Determination of pKa Values for Asp, Glu, His, and Lys Mutants at Each Variable
Contiguous Enzyme-inhibitor Contact Position of the Turkey Ovomucoid Third Domain" Biochemistry 42, 2847-2856 (2003).
PubMed: 12627950
Assembly members:
Turkey Ovomucoid Third Domain, polymer, 56 residues, Formula weight is not available
Natural source: Common Name: Turkey Taxonomy ID: 9103 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Meleagris gallopavo
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
Turkey Ovomucoid Third Domain: LAAVSVDCSEYPKPACVLEY
APLCGSDNKTYGNKCNFCNA
VVESNGTLTLSHFGKC
| Data type | Count |
| pH NMR parameter values | 16 |
| pKa values | 1 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | P2-Val,P3'-Ala OMTKY3 | 1 |
Entities:
Entity 1, P2-Val,P3'-Ala OMTKY3 56 residues - Formula weight is not available
| 1 | LEU | ALA | ALA | VAL | SER | VAL | ASP | CYS | SER | GLU | ||||
| 2 | TYR | PRO | LYS | PRO | ALA | CYS | VAL | LEU | GLU | TYR | ||||
| 3 | ALA | PRO | LEU | CYS | GLY | SER | ASP | ASN | LYS | THR | ||||
| 4 | TYR | GLY | ASN | LYS | CYS | ASN | PHE | CYS | ASN | ALA | ||||
| 5 | VAL | VAL | GLU | SER | ASN | GLY | THR | LEU | THR | LEU | ||||
| 6 | SER | HIS | PHE | GLY | LYS | CYS |
Samples:
sample_1: Turkey Ovomucoid Third Domain 2 mM; KCl 100 mM; DSS 0.4 mM
conditions_set_1: ionic strength: 100 mM; pH: .; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| TOCSY | sample_1 | not available | conditions_set_1 |
Software:
No software information available
NMR spectrometers:
- Bruker DMX 500 MHz