BMRB Entry 53325
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR53325
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
All files associated with the entry
Citation: Han, Min Ae; Ashim, Janbolat; Ji, Youngheum; Kang, Eunho; Jeong, Minchan; Kim, Sung Jae; Yu, Wookyung; Kim, Jin Hae; Moon, Cheil; Lee, Chang-Hun. "Erythropoietin-derived Non-erythropoietic Peptides Conferring Oxidative Stress Resistance to Keratinocytes and Fibroblasts
" Cell Biochem. Biophys. 84, 2145-2154 (2026).
PubMed: 41524842
Assembly members:
entity_1, polymer, 23 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: LQRHVDKRVSGLRSLTTLLR
ALG
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 70 |
| 1H chemical shifts | 147 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Erythropoietin-derived peptide ML1-C1 | 1 |
Entities:
Entity 1, Erythropoietin-derived peptide ML1-C1 23 residues - Formula weight is not available
| 1 | LEU | GLN | ARG | HIS | VAL | ASP | LYS | ARG | VAL | SER | ||||
| 2 | GLY | LEU | ARG | SER | LEU | THR | THR | LEU | LEU | ARG | ||||
| 3 | ALA | LEU | GLY |
Samples:
sample_1: Erythropoietin-derived peptide ML1-C2 mM; D2O 7%; DSS 0.3 mM; sodium chloride 137 mM; potassium chloride 2.7 mM; disodium phosphate 10 mM; monopotassium phosphate 1.8 mM
sample_conditions_1: ionic strength: 0.17 M; pH: 7.4; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H ROESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-13C HSQC | sample_1 | isotropic | sample_conditions_1 |
Software:
NMRFAM-SPARKY - peak picking
NMRFAM-SPARKY - chemical shift assignment
X-PLOR NIH - refinement
NMR spectrometers:
- Bruker AVANCE III HD 850 MHz