BMRB Entry 5268
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR5268
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Fujitani, Naoki; Kawabata, Shun-ichiro; Osaki, Tsukasa; Kumaki, Yasuhiro; Demura, Makoto; Nitta, Katsutoshi; Kawano, Keiichi. "Structure of the Antimicrobial Peptide Tachystatin A" J. Biol. Chem. 277, 23651-23657 (2002).
PubMed: 11959852
Assembly members:
tachystatin A, polymer, 44 residues, 5055.8 Da.
Natural source: Common Name: Japanese horseshoe crab Taxonomy ID: 6853 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Tachypleus tridentatus
Experimental source: Production method: purified from the natural source
Entity Sequences (FASTA):
tachystatin A: YSRCQLQGFNCVVRSYGLPT
IPCCRGLTCRSYFPGSTYGR
CQRY
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 297 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | tachystatin A | 1 |
Entities:
Entity 1, tachystatin A 44 residues - 5055.8 Da.
| 1 | TYR | SER | ARG | CYS | GLN | LEU | GLN | GLY | PHE | ASN | ||||
| 2 | CYS | VAL | VAL | ARG | SER | TYR | GLY | LEU | PRO | THR | ||||
| 3 | ILE | PRO | CYS | CYS | ARG | GLY | LEU | THR | CYS | ARG | ||||
| 4 | SER | TYR | PHE | PRO | GLY | SER | THR | TYR | GLY | ARG | ||||
| 5 | CYS | GLN | ARG | TYR |
Samples:
sample_1: tachystatin A 2.0 mM
exp_cond_1: pH*: 3.0; temperature: 293 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H DQF-COSY | not available | not available | not available |
| 2D 1H-1H E-COSY | not available | not available | not available |
| 2D 1H-1H HOHAHA | not available | not available | not available |
| 2D 1H-1H NOESY | not available | not available | not available |
Software:
XEASY v1.3.13 -
NMR spectrometers:
- JEOL Alpha 500 MHz
- JEOL Alpha 600 MHz
- Bruker DMX 500 MHz