BMRB Entry 52313

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR52313

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Title:
Vcom1
Deposition date:
2024-02-07
Original release date:
2024-07-22
Authors:
Khatibi, Negin; Huang, Yen-Hua; Wang, Conan; Durek, Thomas; Gilding, Edward; Craik, David
Citation:

Citation: Khatibi, Negin; Huang, Yen-Hua; Wang, Conan; Durek, Thomas; Gilding, Edward; Craik, David. "Isolation and Characterization of Insecticidal Cyclotides from Viola communis"  J. Nat. Prod. ., .-. (2024).
PubMed: 38747744

Assembly members:

Assembly members:
entity_1, polymer, 30 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: Violaceae   Taxonomy ID: 24921   Superkingdom: Eukaryota   Kingdom: Viridiplantae   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: purified from the natural source

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity_1: AAVPCGESCVWIPCFSSVIG CSCKNKVCYN

Data sets:
Data typeCount
1H chemical shifts64

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
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Assembly:

Entity Assembly IDEntity NameEntity ID
1Vcom1 monomer1

Entities:

Entity 1, Vcom1 monomer 30 residues - Formula weight is not available

1   ALAALAVALPROCYSGLYGLUSERCYSVAL
2   TRPILEPROCYSPHESERSERVALILEGLY
3   CYSSERCYSLYSASNLYSVALCYSTYRASN

Samples:

sample_1: Vcom1 0.7 mg

sample_conditions_1: ionic strength: 0 M; pH: 3.8; pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1

Software:

TOPSPIN - collection

NMR spectrometers:

  • Bruker ARX 600 600 MHz