BMRB Entry 51754
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR51754
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Citation: Vugmeyster, Liliya; Ostrovsky, Dmitry; Rodgers, Aryana; Gwin, Kirsten; Smirnov, Serge; McKnight, C James; Fu, Riqiang. "Persistence of Methionine Side Chain Mobility at Low Temperatures in a Nine-Residue Low Complexity Peptide, as Probed by 2 H Solid-State NMR" Chemphyschem 25, e202300565-e202300565 (2024).
PubMed: 38175858
Assembly members:
entity_1, polymer, 9 residues, 822.98 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: GGKGMGFGL
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 7 |
| 1H chemical shifts | 53 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | RC9 | 1 |
Entities:
Entity 1, RC9 9 residues - 822.98 Da.
| 1 | GLY | GLY | LYS | GLY | MET | GLY | PHE | GLY | LEU |
Samples:
sample_1: RC9 1.0625 mM
sample_conditions_1: ionic strength: 0 M; pH: 2; pressure: 1 atm; temperature: 285 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-13C HSQC | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H ROESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
NMRPipe v11.1 Rev 2022.214.10.43 - processing
NMRView v9.2-b27 - chemical shift assignment
NMR spectrometers:
- Bruker AVANCE III 500 MHz (1H Larmor frequency) MHz