BMRB Entry 51743

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR51743

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Title:
[D-Cys5,Asp7,Val8,D-Lys16]-STp(5-17), native form
Deposition date:
2022-12-15
Original release date:
2023-03-07
Authors:
Shimamoto, Shigeru; Hidaka, Yuji
Citation:

Citation: Goto, Masaya; Yoshino, Shinya; Hiroshima, Kyona; Kawakami, Toru; Murota, Kaeko; Shimamoto, Shigeru; Hidaka, Yuji. "The Molecular Basis of Heat-Stable Enterotoxin for Vaccine Development and Cancer Cell Detection"  Molecules 28, 1128-1128 (2023).
PubMed: 36770798

Assembly members:

Assembly members:
entity_1, polymer, 13 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: E. coli   Taxonomy ID: 562   Superkingdom: Bacteria   Kingdom: not available   Genus/species: Escherichia coli

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity_1: XCDVCCNPACAXC

Data sets:
Data typeCount
1H chemical shifts60

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1[D-Cys5,Asp7,Val8,D-Lys16]-STp(5-17), native form1

Entities:

Entity 1, [D-Cys5,Asp7,Val8,D-Lys16]-STp(5-17), native form 13 residues - Formula weight is not available

1   DCYCYSASPVALCYSCYSASNPROALACYS
2   ALADLYCYS

Samples:

sample_1: [D-Cys5,Asp7,Val8,D-Lys16]-STp(5-17) 3 mM; sodium phosphate buffer 25 mM

sample_conditions_1: ionic strength: 25 mM; pH: 6.5; pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D DQF-COSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1

Software:

NMRPipe - chemical shift assignment

NMR spectrometers:

  • JEOL JNM-ECA800 800 MHz