BMRB Entry 51691

Title:
1H, 13C, and 15N Chemical Shift Assignments for amyloidogenic SEM1(49-67) peptide
Deposition date:
2022-11-09
Original release date:
2022-11-16
Authors:
Semenova, Evgenia; Yulmetov, Aydar; Osetrina, Daria; Blokhin, Dmitriy
Citation:

Citation: Osetrina, Daria; Kusova, Aleksandra; Bikmullin, Aydar; Klochkova, Evelina; Yulmetov, Aydar; Semenova, Evgenia; Mukhametzyanov, Timur; Usachev, Konstantin; Klochkov, Vladimir; Blokhin, Dmitriy. "Extent of N-Terminus Folding of Semenogelin 1 Cleavage Product Determines Tendency to Amyloid Formation"  Int. J. Mol. Sci. 24, 8949-8949 (2023).
PubMed: 37240295

Assembly members:

Assembly members:
entity_1, polymer, 19 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: Human   Taxonomy ID: 9606   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Homo sapiens

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity_1: SGQKGKQQTESKGSFSIQY

Data sets:
Data typeCount
13C chemical shifts84
15N chemical shifts18
1H chemical shifts135

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1SEM1(49-67)1

Entities:

Entity 1, SEM1(49-67) 19 residues - Formula weight is not available

1   SERGLYGLNLYSGLYLYSGLNGLNTHRGLU
2   SERLYSGLYSERPHESERILEGLNTYR

Samples:

sample_1: SEM1(49-67) 0.8 mM

sample_conditions_1: pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-15N HSQCsample_1isotropicsample_conditions_1
2D 1H-13C HSQCsample_1isotropicsample_conditions_1
2D 1H-1H ROESYsample_1isotropicsample_conditions_1
2D 1H-13C HMBCsample_1isotropicsample_conditions_1

Software:

CcpNmr Analysis v3.1 - chemical shift assignment

NMR spectrometers:

  • Bruker Avance 500 MHz

Download HSQC peak lists in one of the following formats:
CSV: Backbone or all simulated peaks
SPARKY: Backbone or all simulated peaks