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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR51079
MolProbity Validation Chart
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NMR-STAR v3 text file.
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Citation: Jones, Alisha; Tikhaia, Ekaterina; Mourao, Andre; Sattler, Michael. "Structural effects of m6A modification of the Xist A-repeat AUCG tetraloop and its recognition by YTHDC1" Nucleic Acids Res. 50, 2350-2362 (2022).
PubMed: 35166835
Assembly members:
entity_1, polymer, 14 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: enzymatic semisynthesis
Entity Sequences (FASTA):
entity_1: GGCGCXUCGGCGCC
Data type | Count |
13C chemical shifts | 50 |
15N chemical shifts | 8 |
1H chemical shifts | 86 |
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | (m6A)UCG tetraloop hairpin | 1 |
Entity 1, (m6A)UCG tetraloop hairpin 14 residues - Formula weight is not available
1 | G | G | C | G | C | 6MZ | U | C | G | G | ||||
2 | C | G | C | C |
sample_1: Xist (m6A)UCG tetraloop hairpin 1 mM; sodium chloride 25 mM; sodium phosphate 25 mM
sample_2: Xist (m6A)UCG tetraloop hairpin 1 mM; sodium chloride 25 mM; sodium phosphate 25 mM
sample_3: Xist (m6A)UCG tetraloop hairpin, [U-100% 13C; U-100% 15N], 1 mM; sodium chloride 25 mM; sodium phosphate 25 mM
sample_conditions_1: pH: 6.5; pressure: 1 atm; temperature: 298 K
sample_conditions_2: pH: 6.5; pressure: 1 atm; temperature: 280 K
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
2D 1H-1H TOCSY | sample_2 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_2 | isotropic | sample_conditions_1 |
2D 1H-13C HMQC | sample_2 | isotropic | sample_conditions_1 |
3D 1H-13C NOESY-HMQC | sample_3 | isotropic | sample_conditions_1 |
HNN-COSY | sample_3 | isotropic | sample_conditions_1 |
2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_2 |
2D 1H-1H NOESY | sample_2 | isotropic | sample_conditions_2 |
CcpNMR v2.4 - chemical shift assignment
TOPSPIN v3.5 pl6 - collection, processing
X-PLOR NIH v3.1 - refinement, structure solution