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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR5075
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
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Citation: Maderegger, B.; Bermel, W.; Hrzenjak, A.; Kostner, G.; Sterk, H.. "Solution Structure of Human Apolipoprotein(a) Kringle IV type 6" Biochemistry 41, 660-668 (2002).
PubMed: 11781107
Assembly members:
Apolipoprotein(a) kringle IV type6, polymer, 119 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
Apolipoprotein(a) kringle IV type6: ARIHHHHHHIEGRAPTEQSP
GVQDCYHGDGQSYRGSFSTT
VTGRTCQSWSSMTPHWHQRT
TEYYPNGGLTRNYCRNPDAE
ISPWCYTMDPNVRWEYCNLT
QCPVTESSVLATSTAVSEQ
Data type | Count |
13C chemical shifts | 388 |
15N chemical shifts | 110 |
1H chemical shifts | 612 |
Entity Assembly ID | Entity Name | Entity ID |
---|---|---|
1 | Apolipoprotein(a)kringle IV type 6 | 1 |
Entity 1, Apolipoprotein(a)kringle IV type 6 119 residues - Formula weight is not available
1 | ALA | ARG | ILE | HIS | HIS | HIS | HIS | HIS | HIS | ILE | ||||
2 | GLU | GLY | ARG | ALA | PRO | THR | GLU | GLN | SER | PRO | ||||
3 | GLY | VAL | GLN | ASP | CYS | TYR | HIS | GLY | ASP | GLY | ||||
4 | GLN | SER | TYR | ARG | GLY | SER | PHE | SER | THR | THR | ||||
5 | VAL | THR | GLY | ARG | THR | CYS | GLN | SER | TRP | SER | ||||
6 | SER | MET | THR | PRO | HIS | TRP | HIS | GLN | ARG | THR | ||||
7 | THR | GLU | TYR | TYR | PRO | ASN | GLY | GLY | LEU | THR | ||||
8 | ARG | ASN | TYR | CYS | ARG | ASN | PRO | ASP | ALA | GLU | ||||
9 | ILE | SER | PRO | TRP | CYS | TYR | THR | MET | ASP | PRO | ||||
10 | ASN | VAL | ARG | TRP | GLU | TYR | CYS | ASN | LEU | THR | ||||
11 | GLN | CYS | PRO | VAL | THR | GLU | SER | SER | VAL | LEU | ||||
12 | ALA | THR | SER | THR | ALA | VAL | SER | GLU | GLN |
sample_1: Apolipoprotein(a) kringle IV type6, [U-15N], 0.7 mM; phosphate buffer 15 mM; NaCl 50 mM; H2O 90%; D2O 10%
sample_2: Apolipoprotein(a) kringle IV type6, [U-15N; U-13C], 0.7 mM; phosphate buffer 15 mM; NaCl 50 mM; H2O 90%; D2O 10%
sample_cond_1: ionic strength: 65 mM; pH: 6.5; pressure: 1 atm; temperature: 303 K
Name | Sample | Sample state | Sample conditions |
---|---|---|---|
3D 15N-separated NOESY | not available | not available | not available |
3D 13C-separated NOESY | not available | not available | not available |
HNHA | not available | not available | not available |
NMRPipe v1.6 - processing
ANSIG v3.3 - data analysis
XWINNMR v2.6 - collection
X-PLOR v3.0 - refinement, structure solution
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