BMRB Entry 4926

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4926

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Title:
1H and 15N Chemical Shifts of CI2 with a ten glutamine repeat between residues 59 and 60
Deposition date:
2000-12-15
Original release date:
2001-03-06
Authors:
Gordon-Smith, Duncan; Stott, Kelvin; Carbajo, Rodrigo; Neuhaus, David
Citation:

Citation: Gordon-Smith, Duncan; Carbajo, Rodrigo; Stott, Kelvin; Neuhaus, David. "Solution studies of chymotrypsin inhibitor-2 glutamine insertion mutants show no interglutamine interactions"  Biochem. Biophys. Res. Commun. 280, 855-860 (2001).

Assembly members:

Assembly members:
Chymotrypsin inhibitor 2, polymer, 76 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: E. coli   Taxonomy ID: 562   Superkingdom: Bacteria   Kingdom: not available   Genus/species: Escherichia coli

Experimental source:

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):

Entity Sequences (FASTA):
Chymotrypsin inhibitor 2: KTEWPELVGKSVEEAKKVIL QDKPEAQIIVLPVGTIVTMG QQQQQQQQQQGMEYRIDRVR LFVDKLDNIAQVPRVG

Data sets:
Data typeCount
15N chemical shifts123
1H chemical shifts498

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1ci21

Entities:

Entity 1, ci2 76 residues - Formula weight is not available

1   LYSTHRGLUTRPPROGLULEUVALGLYLYS
2   SERVALGLUGLUALALYSLYSVALILELEU
3   GLNASPLYSPROGLUALAGLNILEILEVAL
4   LEUPROVALGLYTHRILEVALTHRMETGLY
5   GLNGLNGLNGLNGLNGLNGLNGLNGLNGLN
6   GLYMETGLUTYRARGILEASPARGVALARG
7   LEUPHEVALASPLYSLEUASPASNILEALA
8   GLNVALPROARGVALGLY

Samples:

sample_1: Chymotrypsin inhibitor 2, [U-90% 15N], mM

Ex-cond_1: pH: 4.6; temperature: 315 K

Ex-cond_2: pH: 4.6; temperature: 300 K

Experiments:

NameSampleSample stateSample conditions

Software:

No software information available

NMR spectrometers:

  • unknown unknown 0 MHz

Related Database Links:

PDB

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