BMRB Entry 4741
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4741
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Citation: Chang, Xiaoqing; Keller, D; Bjorn, S.; Led, Jens. "Structure and folding of Glucagon-like Peptide 1-7-(7-36)-amide in aqueous trifluoroethanol studied by NMR" Magn. Reson. Chem. 39, 477-483 (2001).
Assembly members:
Glucogen-like peptide-1-(7-36)-amide, polymer, 30 residues, 3300 Da.
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
Glucogen-like peptide-1-(7-36)-amide: HAEGTFTSDVSSYLEGQAAK
EFIAWLVKGR
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 1512 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | GLP-1 | 1 |
Entities:
Entity 1, GLP-1 30 residues - 3300 Da.
| 1 | HIS | ALA | GLU | GLY | THR | PHE | THR | SER | ASP | VAL | |
| 2 | SER | SER | TYR | LEU | GLU | GLY | GLN | ALA | ALA | LYS | |
| 3 | GLU | PHE | ILE | ALA | TRP | LEU | VAL | LYS | GLY | ARG |
Samples:
sample_1: Glucogen-like peptide-1-(7-36)-amide 1.4 mM
sample_2: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 4.62%
sample_3: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 8.82%
sample_4: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 13.89%
sample_5: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 19.48%
sample_6: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 24.39%
sample_7: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 29.55%
sample_8: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 34.74%
sample_9: Glucogen-like peptide-1-(7-36)-amide 1.4 mM; 2,2,2-trifluoroethanol-d3 50%
cond-1: pH*: 2.50; temperature: 300 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| PFG self-diffusion experiment with water-sLED pulse | not available | not available | not available |
| NOESY | not available | not available | not available |
| TOCSY | not available | not available | not available |
Software:
No software information available
NMR spectrometers:
- Varian Inova Plus 500 MHz
- Varian Inova Plus 750 MHz
- Bruker AM 500 MHz