BMRB Entry 4565
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR4565
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Citation: Feng, Yiqing; Likos, John; Zhu, Leiming; Woodward, Harold; McDonald, Joseph; Stevens, Anna; Howard, Susan; Welsch, Dean. "Letter to the Editor: 1H, 13C and 15N resonance assignments for a
truncated and inhibited catalytic domain of matrix metalloproteinase-2" J. Biomol. NMR 17, 85-86 (2000).
Assembly members:
mmp2, polymer, 163 residues, 18461 Da.
I52, non-polymer, 574.732 Da.
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 610 |
| 15N chemical shifts | 144 |
| 1H chemical shifts | 945 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | mmp2 | 1 |
| 2 | inhibitor | 2 |
Entities:
Entity 1, mmp2 163 residues - 18461 Da.
| 1 | MET | TYR | ASN | PHE | PHE | PRO | ARG | LYS | PRO | LYS | ||||
| 2 | TRP | ASP | LYS | ASN | GLN | ILE | THR | TYR | ARG | ILE | ||||
| 3 | ILE | GLY | TYR | THR | PRO | ASP | LEU | ASP | PRO | GLU | ||||
| 4 | THR | VAL | ASP | ASP | ALA | PHE | ALA | ARG | ALA | PHE | ||||
| 5 | GLN | VAL | TRP | SER | ASP | VAL | THR | PRO | LEU | ARG | ||||
| 6 | PHE | SER | ARG | ILE | HIS | ASP | GLY | GLU | ALA | ASP | ||||
| 7 | ILE | MET | ILE | ASN | PHE | GLY | ARG | TRP | GLU | HIS | ||||
| 8 | GLY | ASP | GLY | TYR | PRO | PHE | ASP | GLY | LYS | ASP | ||||
| 9 | GLY | LEU | LEU | ALA | HIS | ALA | PHE | ALA | PRO | GLY | ||||
| 10 | THR | GLY | VAL | GLY | GLY | ASP | SER | HIS | PHE | ASP | ||||
| 11 | ASP | ASP | GLU | LEU | TRP | THR | ASN | THR | SER | ALA | ||||
| 12 | ASN | TYR | SER | LEU | PHE | LEU | VAL | ALA | ALA | HIS | ||||
| 13 | GLU | PHE | GLY | HIS | ALA | MET | GLY | LEU | GLU | HIS | ||||
| 14 | SER | GLN | ASP | PRO | GLY | ALA | LEU | MET | ALA | PRO | ||||
| 15 | ILE | TYR | THR | TYR | THR | LYS | ASN | PHE | ARG | LEU | ||||
| 16 | SER | GLN | ASP | ASP | ILE | LYS | GLY | ILE | GLN | GLU | ||||
| 17 | LEU | TYR | GLY |
Entity 2, inhibitor - C29 H42 N4 O6 S - 574.732 Da.
| 1 | I52 |
Samples:
sample_1: mmp2, [U-13C; U-15N], 0.35 mM
sample_conditions_set_1: pH: 7.4; pressure: 1 atm; temperature: 303 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| not available | sample_1 | not available | sample_conditions_set_1 |
Software:
No software information available
NMR spectrometers:
- unknown unknown 0 MHz
Download HSQC peak lists in one of the following formats:
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