BMRB Entry 4243
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4243
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: GALLEGO, JOSE; CHOU, SHAN-HO; REID, BRIAN. "Centromeric pyrimidine strands fold into an intercalated motif by forming a
double hairpin with a novel T:G:G:T tetrad: solution structure of the
D(TCCCGTTTCCA) dimer" J. Mol. Biol. 273, 840-856 (1997).
Assembly members:
DNA_1, polymer, 11 residues, Formula weight is not available
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
DNA_1: TCCCGTTTCCA
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 84 |
| 31P chemical shifts | 10 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | DNA monomer 1 | 1 |
| 2 | DNA monomer 2 | 1 |
Entities:
Entity 1, DNA monomer 1 11 residues - Formula weight is not available
| 1 | DT | DC | DC | DC | DG | DT | DT | DT | DC | DC | ||||
| 2 | DA |
Samples:
sample_one: DNA_1 3.9 mM
sample_conditions_one: ionic strength: 0.2 M; pH: 4.1; temperature: 302 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1D H | sample_one | not available | sample_conditions_one |
| 1D P | sample_one | not available | sample_conditions_one |
| 2D H/H NOESY | sample_one | not available | sample_conditions_one |
| H/H COSY | sample_one | not available | sample_conditions_one |
| H/P HETCOR | sample_one | not available | sample_conditions_one |
Software:
FELIX v2.30 -
DISCOVER -
AMBER v4.0 -
BIRDER - relaxation matrix simulation
NMR spectrometers:
- Bruker DMX 750 MHz
- Home-built . 500 MHz