BMRB Entry 397
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR397
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Citation: Heitz, Annie; Chiche, Laurent; Le-Nguyen, Dung; Castro, Bertrand. "1H 2D NMR and Distance Geometry Study of the Folding of Ecballium elaterium
Trypsin Inhibitor, a Member of the Squash Inhibitors Family" Biochemistry 28, 2392-2398 (1989).
PubMed: 2730872
Assembly members:
EETI-II, polymer, 28 residues, Formula weight is not available
Natural source: Common Name: Jumping cucumber Taxonomy ID: 3679 Superkingdom: Eukaryota Kingdom: Virdiplanta Genus/species: Ecballium elaterium
Experimental source: Production method: synthetic
Entity Sequences (FASTA):
EETI-II: GCPRILMRCKQDSDCLAGCV
CGPNGFCG
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 81 |
| 1H chemical shifts | 174 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | EETI-II | 1 |
Entities:
Entity 1, EETI-II 28 residues - Formula weight is not available
| 1 | GLY | CYS | PRO | ARG | ILE | LEU | MET | ARG | CYS | LYS | ||||
| 2 | GLN | ASP | SER | ASP | CYS | LEU | ALA | GLY | CYS | VAL | ||||
| 3 | CYS | GLY | PRO | ASN | GLY | PHE | CYS | GLY |
Samples:
sample_1: EETI-II 4.0 mM
sample_cond_1: pH: 2.7; pressure: 1 atm; temperature: 290 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | isotropic | not available |
| COSY | not available | isotropic | not available |
| TOCSY | not available | isotropic | not available |
| 1H-13C HSQC | not available | isotropic | not available |
| 1H-13C HSQC-TOCSY | not available | isotropic | not available |
Software:
xwinnmr v3.1 -
NMR spectrometers:
- Bruker Avance 600 MHz