BMRB Entry 34306
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR34306
MolProbity Validation Chart
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NMR-STAR v3 text file.
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Citation: Prior, S.. "Trpzip2 structure in presence of exogenous haloprotectant molecule." .
Assembly members:
entity_1, polymer, 13 residues, 1608.776 Da.
Natural source: Common Name: not available Taxonomy ID: 32630 Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: SWTWENGKWTWKX
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 40 |
| 1H chemical shifts | 92 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity_1 | 1 |
Entities:
Entity 1, entity_1 13 residues - 1608.776 Da.
| 1 | SER | TRP | THR | TRP | GLU | ASN | GLY | LYS | TRP | THR | ||||
| 2 | TRP | LYS | NH2 |
Samples:
sample_1: Trpzip2 2 mM; potassium phosphate 50 mM; ectoine 250 mM
sample_conditions_1: ionic strength: 50 mM; pH: 5.5; pressure: 1 atm; temperature: 300 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
TopSpin, Bruker Biospin - collection
CcpNmr Analysis, CCPN - chemical shift assignment
CNS, Brunger, Adams, Clore, Gros, Nilges and Read - structure calculation
NMR spectrometers:
- Bruker AVANCE III 500 MHz