BMRB Entry 34186
Click here to enlarge.
PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR34186
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Karg, B.; Weisz, K.. "Loop Length Affects Syn-Anti Conformational Rearrangements in Parallel G-Quadruplexes." Chemistry 24, 10246-10252 (2018).
PubMed: 29756658
Assembly members:
entity_1, polymer, 22 residues, 7324.094 Da.
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: TGAXGGTXGGTAXGGTXGGT
AA
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 158 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity_1 | 1 |
Entities:
Entity 1, entity_1 22 residues - 7324.094 Da.
| 1 | DT | DG | DA | BGM | DG | DG | DT | BGM | DG | DG | ||||
| 2 | DT | DA | BGM | DG | DG | DT | BGM | DG | DG | DT | ||||
| 3 | DA | DA |
Samples:
sample_1: entity_1 mM; potassium phosphate 10 mM
sample_2: entity_1 mM; potassium phosphate 10 mM
sample_conditions_1: ionic strength: 10 mM; pH: 7 pH*; pressure: 1 atm; temperature: 303 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_2 | isotropic | sample_conditions_1 |
Software:
AMBER, Case, Darden, Cheatham III, Simmerling, Wang, Duke, Luo, ... and Kollman - refinement, structure calculation
X-PLOR NIH, Schwieters, Kuszewski, Tjandra and Clore - structure calculation
CcpNMR, CCPN - chemical shift assignment, peak picking
NMR spectrometers:
- Bruker Avance 600 MHz