BMRB Entry 25478
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full, SPARTA
BMRB Entry DOI: doi:10.13018/BMR25478
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
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Citation: Ganjiwale, Anjali; Eldeeb, Khalil; Chandrashekaran, Indu; Cowsik, Sudha; Howlett, Allyn. "Phosphorylation of CB1Cannabinoid Receptor Fourth Intracellular Loop Pepducins:
Effects on Structure and Function" J. Biol. Chem. ., .-..
Assembly members:
entity, polymer, 17 residues, 2136.324 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity: RSKDLRHAFRXMFPSSE
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 84 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity | 1 |
Entities:
Entity 1, entity 17 residues - 2136.324 Da.
| 1 | ARG | SER | LYS | ASP | LEU | ARG | HIS | ALA | PHE | ARG | ||||
| 2 | SEP | MET | PHE | PRO | SER | SER | GLU |
Samples:
sample_1: IL4pSER411 peptide 5 mM; SDS, [U-100% 2H], 72 mM; D2O 10%; H2O 90%
sample_conditions_1: ionic strength: 5 mM; pH: 4.5; pressure: 1 atm; temperature: 310 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
No software information available
NMR spectrometers:
- Bruker DRX 500 MHz