BMRB Entry 25207
Click here to enlarge.
PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR25207
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Espejo, Fabiola; Cubillos, Marcia; Salazar, Luz Mary; Guzman, Fanny; Urquiza, Mauricio; Ocampo, Marisol; Silva, Yolanda; Rodriguez, Raul; Lioy, Eduardo; Patarroyo, Manuel Elkin. "Structure Immunogenicity and Proctivity Relationship for the 1585 Malarial Peptide and Its Substitution Analogues" Angew. Chem. Int. Ed. 40, 4654-4657 (2001).
PubMed: 12404375
Assembly members:
entity, polymer, 20 residues, 2351.851 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity: EVLYLKPLAGVYRSLKKQLE
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 176 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Malarial Peptide | 1 |
Entities:
Entity 1, Malarial Peptide 20 residues - 2351.851 Da.
| 1 | GLU | VAL | LEU | TYR | LEU | LYS | PRO | LEU | ALA | GLY | |
| 2 | VAL | TYR | ARG | SER | LEU | LYS | LYS | GLN | LEU | GLU |
Samples:
sample_1: TFE 8 mM
sample_conditions_1: temperature: 295 K; pH: 3.7; pressure: 1 atm
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
InsightII, Accelrys Software Inc. - geometry optimization, refinement
NMR spectrometers:
- Bruker DRX 600 MHz