BMRB Entry 25190
Click here to enlarge.
PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR25190
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Cubillos, Marcia; Salazar, Luz Mary; Torres, Libardo; Patarroyo, Manuel Elkin. "Protection against experimental P. falciparum malaria is associated with short AMA-1 peptide analogue alpha-helical structures" Biochemie 84, 1181-1188 (2002).
PubMed: 12628294
Assembly members:
entity, polymer, 21 residues, 2271.702 Da.
Natural source: Common Name: malaria parasite Taxonomy ID: 5833 Superkingdom: Eukaryota Kingdom: not available Genus/species: Plasmodium falciparum
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity: MIKSAFLPTGAFKADRYKSH
X
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 134 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity | 1 |
Entities:
Entity 1, entity 21 residues - 2271.702 Da.
| 1 | MET | ILE | LYS | SER | ALA | PHE | LEU | PRO | THR | GLY | ||||
| 2 | ALA | PHE | LYS | ALA | ASP | ARG | TYR | LYS | SER | HIS | ||||
| 3 | NH2 |
Samples:
sample_1: entity 8 mM; water 70%; trifluoroethanol 30%
sample_conditions_1: pH: 3.7; pressure: 1 atm; temperature: 295 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
InsightII, Accelrys Software Inc. - geometry optimization, refinement
NMR spectrometers:
- Bruker DRX 500 MHz