BMRB Entry 21079

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR21079

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Title:
Influenza Hemagglutinin Peptide
Deposition date:
2017-07-03
Original release date:
2017-11-10
Authors:
Caffrey, Michael
Citation:

Citation: Caffrey, Michael. "Influenza Hemagglutinin Peptide"  JBC ., .-..

Assembly members:

Assembly members:
entity, polymer, 17 residues, 2020.262 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity: WSYNAELLVAMENQHTI

Data sets:
Data typeCount
13C chemical shifts51
1H chemical shifts102

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1Influenza Hemagglutinin Peptide1

Entities:

Entity 1, Influenza Hemagglutinin Peptide 17 residues - 2020.262 Da.

1   TRPSERTYRASNALAGLULEULEUVALALA
2   METGLUASNGLNHISTHRILE

Samples:

sample_1: peptide mM; sodium phosphate 20 mM; sodium chloride 150 mM; D2O10 – 100%; TFE 40%

sample_conditions_1: pH: 7.5; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-13C HSQCsample_1isotropicsample_conditions_1
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1

Software:

NMRDraw, Delaglio, Zhengrong and Bax - chemical shift assignment

CNS, Brunger, Adams, Clore, Gros, Nilges and Read - structure solution

NMRPipe, Delaglio, Zhengrong and Bax - processing

NMR spectrometers:

  • Bruker Avance 900 MHz