BMRB Entry 21025
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR21025
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Citation: Shoshan, Michal; Shalev, Deborah; Tshuva, Edit. "Peptide Models of Cu(I) and Zn(II) Metallochaperones: The Effect of pH on Coordination and Mechanistic Implications." Inorg. Chem. 52, 2993-3000 (2013).
PubMed: 23458158
Assembly members:
MDCSGCSRPG+Zn, polymer, 10 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
MDCSGCSRPG+Zn: MDCSGCSRPG
- assigned_chemical_shifts
- conformer_family_coord_set
| Data type | Count |
| 1H chemical shifts | 48 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | MDCSGCSRPG | 1 |
Entities:
Entity 1, MDCSGCSRPG 10 residues - Formula weight is not available
| 1 | MET | ASP | CYS | SER | GLY | CYS | SER | ARG | PRO | GLY |
Samples:
sample_1: MDCSGCSRPG 4.0 mM; ZnCl2 4.0 mM; DMSO, [U-2H], 90%; H2O 10%
sample_conditions_1: pH*: 3.0; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
TOPSPIN v1.3, Bruker Biospin, Chimera UCSF, Goddard, Koradi, Billeter and Wuthrich, Schwieters, Kuszewski, Tjandra and Clore - chemical shift assignment, collection, data analysis, peak picking, processing, refinement, structure solution
NMR spectrometers:
- Bruker AVANCE DMX 600 MHz