BMRB Entry 21002

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR21002

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Title:
Solution NMR structure of TZ2C-BG
Deposition date:
2011-03-11
Original release date:
2012-08-07
Authors:
McElheny, Dan; Keiderling, Timothy
Citation:

Citation: Wu, Ling; McElheny, Dan; Setnicka, Vladimir; Hilario, Jovencio; Keiderling, Timothy. "Role of different beta-turns in beta-hairpin conformation and stability studied by optical spectroscopy"  (2012).
PubMed: 21989967

Assembly members:

Assembly members:
TrpZip2c-BG, polymer, 13 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
TrpZip2c-BG: AWAWEXGKWAWKX

Data sets:
Data typeCount
1H chemical shifts87
coupling constants10

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1TrpZip2c-BG1

Entities:

Entity 1, TrpZip2c-BG 13 residues - Formula weight is not available

1   ALATRPALATRPGLUAIBGLYLYSTRPALA
2   TRPLYSNH2

Samples:

sample_1: TrpZip2c-BG4 – 4.1 mM; sodium phosphate 20 mM; H2O 90%; D2O 10%

sample_conditions_1: ionic strength: 0.02 M; pH: 5.8; pressure: 1 atm; temperature: 283 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1
2D 1H-1H COSYsample_1isotropicsample_conditions_1

Software:

CYANA v2.0, Guntert, Mumenthaler and Wuthrich - structure solution

NMR spectrometers:

  • Bruker Avance 800 MHz