BMRB Entry 20128
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20128
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Hong, Jing; Lin, Donghai. "Solution structure of conotoxin qc16a" .
Assembly members:
conotoxin_qc16a, polymer, 11 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
conotoxin_qc16a: DCQPCGHNVCC
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 47 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | conotoxin qc16a | 1 |
Entities:
Entity 1, conotoxin qc16a 11 residues - Formula weight is not available
| 1 | ASP | CYS | GLN | PRO | CYS | GLY | HIS | ASN | VAL | CYS | ||||
| 2 | CYS |
Samples:
sample_1: conotoxin qc16a 4 mM; H2O 90%; D2O 10%
sample_2: conotoxin qc16a 4 mM; D2O 100%
sample_conditions_1: pH: 3.5; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY no.1 | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY no.1 | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY no.2 | sample_2 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY no.2 | sample_2 | isotropic | sample_conditions_1 |
Software:
SPARKY v3.11, Goddard - chemical shift assignment
ARIA v2.2, Linge, O'Donoghue and Nilges - chemical shift assignment
CNS v1.1, Brunger, Adams, Clore, Gros, Nilges and Read - structure solution
NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing
NMR spectrometers:
- Varian INOVA 600 MHz