BMRB Entry 20095
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20095
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Citation: Kim, Jin-Kyoung; Lee, Sung-Ah; Shin, Soyoung; Lee, Jee-Young; Jeong, Ki-Woong; Nan, Yong Hae; Park, Yong Sun; Shin, Song Yub; Kim, Yangmee. "Structural flexibility and the positive charges are the key factors in bacterial cell selectivity and membrane penetration of peptoid-substituted analog of Piscidin 1." Biochim. Biophys. Acta 1798, 1913-1925 (2010).
PubMed: 20603100
Assembly members:
cis Pis-1[NkG], polymer, 22 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
cis Pis-1[NkG]: FFHHIFRXIVHVGKTIHRLV
TG
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 159 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | cis Pis-1[NkG] | 1 |
Entities:
Entity 1, cis Pis-1[NkG] 22 residues - Formula weight is not available
| 1 | PHE | PHE | HIS | HIS | ILE | PHE | ARG | X | ILE | VAL | ||||
| 2 | HIS | VAL | GLY | LYS | THR | ILE | HIS | ARG | LEU | VAL | ||||
| 3 | THR | GLY |
Samples:
sample_1: cis Pis-1[NkG]1 – 2 mM; H2O 90%; D2O 10%
sample_conditions_1: pH: 4.1; temperature: 313 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
Software:
X-PLOR, Brunger - structure solution
NMR spectrometers:
- Bruker DMX 600 MHz
- Bruker Avance 400 MHz