BMRB Entry 20058
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20058
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Citation: Bhunia, Anirban; Mohanram, Harini; Domadia, Prerna; Torres, Jaume; Bhattacharjya, Surajit. "Designed beta-boomerang antiendotoxic and antimicrobial peptides: structures and activities in lipopolysaccharide" J. Biol. Chem. 284, 21991-22004 (2009).
PubMed: 19520860
Assembly members:
YI12WW, polymer, 12 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
YI12WW: YVLWKRKRWIFI
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 85 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | YI12WW | 1 |
Entities:
Entity 1, YI12WW 12 residues - Formula weight is not available
| 1 | TYR | VAL | LEU | TRP | LYS | ARG | LYS | ARG | TRP | ILE | ||||
| 2 | PHE | ILE |
Samples:
sample_1: YI12WW 0.5 ± 0.02 mM; H2O 90%; D2O 10%
sample_conditions_1: pH: 4.5; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H trNOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
DYANA v1.5, Guntert, Braun and Wuthrich - refinement
NMR spectrometers:
- Bruker DRX 600 MHz