BMRB Entry 20028
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20028
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Citation: Guo, Syuan-Ming. "." J. Biomol. NMR ., .-..
Assembly members:
Statherin, polymer, 15 residues, 1958 Da.
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
Statherin: DXXEEKFLRRIGRFG
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 94 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity_1 | 1 |
| 2 | entity_2 | 1 |
| 3 | entity_3 | 1 |
| 4 | entity_4 | 1 |
| 5 | entity_5 | 1 |
| 6 | entity_6 | 1 |
| 7 | entity_7 | 1 |
| 8 | entity_8 | 1 |
| 9 | entity_9 | 1 |
| 10 | entity_10 | 1 |
Entities:
Entity 1, entity_1 15 residues - 1958 Da.
| 1 | ASP | SEP | SEP | GLU | GLU | LYS | PHE | LEU | ARG | ARG | ||||
| 2 | ILE | GLY | ARG | PHE | GLY |
Samples:
sample_1: statherin 1-15 polypeptide1 – 3 mM
sample_conditions_1: pH: 6; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
ARIA, Linge, O'Donoghue and Nilges - geometry optimization
NMR spectrometers:
- Bruker DRX 600 MHz