BMRB Entry 20001
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR20001
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Citation: Li, Jianxu; Wu, Hongbing; Hong, Jing; Xu, Xueqing; Yang, Hailong; Wu, Bingxian; Wang, Yipeng; Zhu, Jianhua; Lai, Ren; Jiang, Xinguo; Lin, Donghai; Prescott, Mark; Rees, Huw. "odorranalectin is a small peptide lectin with potential for drug delivery and targeting" PLoS ONE 3, .-. (2008).
PubMed: 18584053
Assembly members:
odorranalectin, polymer, 17 residues, 1888.21 Da.
Natural source: Common Name: Yunnanfu frog Taxonomy ID: 167935 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Odorrana grahami
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
odorranalectin: YASPKCFRYPNGVLACT
- assigned_chemical_shifts
- coupling_constants
- homonucl_NOEs
| Data type | Count |
| 1H chemical shifts | 104 |
| coupling constants | 12 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | odorranalectin | 1 |
Entities:
Entity 1, odorranalectin 17 residues - 1888.21 Da.
| 1 | TYR | ALA | SER | PRO | LYS | CYS | PHE | ARG | TYR | PRO | ||||
| 2 | ASN | GLY | VAL | LEU | ALA | CYS | THR |
Samples:
sample_1: odorranalectin peptide 3 mM; sodium phosphate 20 mM; sodium chloride 100 mM; H2O 90%; D2O 10%
sample_conditions_1: ionic strength: 100 mM; pH: 6.0; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
ARIA v2.2, Linge, O'Donoghue and Nilges - chemical shift assignment
SPARKY v3.112, Goddard - chemical shift assignment
CNS v1.1, Brunger, Adams, Clore, Gros, Nilges and Read - refinement, structure solution
NMR spectrometers:
- Varian INOVA 600 MHz