BMRB Entry 19923
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR19923
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Citation: Green, Brad; Zhang, Min-Min; Chhabra, Sandeep; Robinson, Samuel; Wilson, Michael; Redding, Addison; Olivera, Baldomero; Yoshikami, Doju; Bulaj, Grzegorz; Norton, Raymond. "Interactions of disulfide-deficient selenocysteine analogs of mu-conotoxin BuIIIB with the alpha-subunit of the voltage-gated sodium channel subtype 1.3" FEBS J 281, 2885-2898 (2014).
PubMed: 24814369
Assembly members:
BuIIIB[C5U,C17U,C6A,C23A], polymer, 24 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
BuIIIB[C5U,C17U,C6A,C23A]: VGERXAKNGKRGCGRWXRDH
SRAC
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 125 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | BuIIB[C5U,C17U,C6A,C23A] | 1 |
Entities:
Entity 1, BuIIB[C5U,C17U,C6A,C23A] 24 residues - Formula weight is not available
| 1 | VAL | GLY | GLU | ARG | SEC | ALA | LYS | ASN | GLY | LYS | ||||
| 2 | ARG | GLY | CYS | GLY | ARG | TRP | SEC | ARG | ASP | HIS | ||||
| 3 | SER | ARG | ALA | CYS |
Samples:
sample_1: BuIIIB[C5U,C17U,C6A,C23A] 160 uM; H2O 95%; D2O 5%
sample_conditions_1: pH: 5.5; pressure: 1 atm; temperature: 273 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
Analysis, CCPN - chemical shift assignment
NMR spectrometers:
- Bruker DRX 600 MHz