BMRB Entry 19580
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full, SPARTA
BMRB Entry DOI: doi:10.13018/BMR19580
MolProbity Validation Chart
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NMR-STAR v3 text file.
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Citation: Blokhin, Dmitriy. "PAP262-270 in SDS micelles" .
Assembly members:
entity_1, polymer, 11 residues, 1051.228 Da.
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: XVLVNEILNHX
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 80 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | PAP262-270 in SDS micelles | 1 |
Entities:
Entity 1, PAP262-270 in SDS micelles 11 residues - 1051.228 Da.
| 1 | ACE | VAL | LEU | VAL | ASN | GLU | ILE | LEU | ASN | HIS | ||||
| 2 | NH2 |
Samples:
sample_1: PAP262-270 300 uM; SDS 50 mM; H2O 90%; D2O 10%
sample_conditions_1: temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
X-PLOR NIH, Schwieters, Kuszewski, Tjandra and Clore - structure solution
SPARKY, Goddard - chemical shift assignment
NMR spectrometers:
- Bruker Avance 500 MHz