BMRB Entry 19469

Title:
Fragment based approach and binding behavior of LFampinB with Lipopolysaccharide: biophysical aspects
Deposition date:
2013-08-29
Original release date:
2013-09-23
Authors:
Bhunia, Anirban; Chatterjee, Subhrangsu; Ghosh, Anirban; Jana, Jagannath
Citation:

Citation: Bhunia, Anirban; Chatterjee, Subhrangsu; Ghosh, Anirban; Jana, Jagannath. "Fragment based approach and binding behaviour of LFampinB with Lipopolysaccharide: biophysical aspects"  .

Assembly members:

Assembly members:
entity, polymer, 10 residues, 1233.493 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
entity: WKLLSKAQEK

Data sets:
Data typeCount
1H chemical shifts65

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1WK10_LPS1

Entities:

Entity 1, WK10_LPS 10 residues - 1233.493 Da.

1   TRPLYSLEULEUSERLYSALAGLNGLULYS

Samples:

sample_1: WK10_LPS 1 mM; H2O 90%; D2O 10%

sample_conditions_1: pH: 4.5; pressure: 1 atm; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H NOESYsample_1isotropicsample_conditions_1

Software:

CYANA v2.1, Guntert, Mumenthaler and Wuthrich - structure solution

NMR spectrometers:

  • Bruker Avance 500 MHz