BMRB Entry 18616

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR18616

NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry

Nicholas Rego and David Koes
3Dmol.js: molecular visualization with WebGL
Bioinformatics (2015) 31 (8): 1322-1324 doi:10.1093/bioinformatics/btu829

Select model:

I am color blind

Download raw data. Direct link to this display. Help

Title:

Relaxation rates for accurate spectral density mapping for unbiased analysis of nucleic acid motions probed by carbon-13 NMR relaxation

Deposition date:

2012-07-26

Original release date:

2019-08-30

Authors:

Kaderavek, Pavel; Zapletal, Vojtech; Fiala, Radovan; Sklenar, Vladimir; Zidek, Lukas

Citation:

Citation: Kaderavek, Pavel; Zapletal, Vojtech; Fiala, Radovan; Srb, Pavel; Padrta, Petr; Precechtelova, Jana Pavlikova; Soltesova, Maria; Kowalewski, Jozef; Widmalm, Goran; Chmelik, Josef; Sklenar, Vladimir; Zidek, Lukas. "Spectral density mapping at multiple magnetic fields suitable for (13)C NMR relaxation studies" J. Magn. Reson. 266, 23-40 (2016).
PubMed: 27003380

Assembly members:

Assembly members:
UUCG_tetraloop, polymer, 14 residues, Formula weight is not available

Natural source:

Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available

Experimental source:

Experimental source: Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
UUCG_tetraloop: GGCACUUCGGUGCC

Data sets:

Data type	Count
T1 relaxation values	39
T1rho relaxation values	39
dipole-CSA cross correlation relaxation values	73
heteronuclear NOE values	52

Additional metadata:

Assembly
Samples and Experiments
Software
Spectrometers
Hide all

Assembly:

Entity Assembly ID	Entity Name	Entity ID
1	UUCG teraloop	1

Entities:

Entity 1, UUCG teraloop 14 residues - Formula weight is not available

1

G

C

A

C

U

C

G

2

U

G

C

Samples:

sample_1: UUCG tetraloop, [U-13C; U-15N], 3.0 mM; EDTA 0.2 mM; sodium phosphate 10 mM; sodium azide 0.05%

sample_conditions_1: pH*: 6.7; pressure: 1 atm; temperature: 298.15 K

Experiments:

Name	Sample	Sample state	Sample conditions
2D R1 13C,1H correlation	sample_1	isotropic	sample_conditions_1
2D R1rho 13C,1H correlation	sample_1	isotropic	sample_conditions_1
2D NOE 13C,1H correlation	sample_1	isotropic	sample_conditions_1
2D constant-time 13C(coupled),1H correlation	sample_1	isotropic	sample_conditions_1

Software:

NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing

SPARKY, Goddard - data analysis

NMR spectrometers:

Varian Unity 400 MHz
Varian Unity 500 MHz
Varian Unity 600 MHz