BMRB Entry 17980
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR17980
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NMR-STAR v3 text file.
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Citation: Do, Ngoc Quang; Phan, Anh Tuan. "Monomer-dimer equilibrium for the 5'-5' stacking of propeller-type parallel-stranded G-quadruplexes: NMR structural study." Chemistry 18, 14752-14759 (2012).
PubMed: 23019076
Assembly members:
DNA_(5'-D(*TP*TP*GP*GP*GP*TP*GP*GP*GP*TP*GP*GP*GP*TP*GP*GP*GP*T)-3')_, polymer, 18 residues, 5730.718 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
DNA_(5'-D(*TP*TP*GP*GP*GP*TP*GP*GP*GP*TP*GP*GP*GP*TP*GP*GP*GP*T)-3')_: TTGGGTGGGTGGGTGGGT
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 159 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | G-quadruplexes | 1 |
Entities:
Entity 1, G-quadruplexes 18 residues - 5730.718 Da.
| 1 | DT | DT | DG | DG | DG | DT | DG | DG | DG | DT | ||||
| 2 | DG | DG | DG | DT | DG | DG | DG | DT |
Samples:
sample_1: G-quadruplexes 0.5 mM; H2O 90%; D2O 10%
sample_conditions_1: ionic strength: 16 mM; pH: 7.0; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
X-PLOR NIH, Schwieters, Kuszewski, Tjandra and Clore - data analysis, geometry optimization, refinement
NMR spectrometers:
- Bruker AMX 600 MHz