BMRB Entry 16287

Title:
d(AGAGCTCT)2 plus dqdppn 1:2 assignments
Deposition date:
2009-05-07
Original release date:
2010-01-28
Authors:
Waywell, Phil; Thomas, James
Citation:

Citation: Waywell, Philip; Thomas, James; Williamson, Mike. "Structural analysis of the binding of the diquaternary pyridophenazine derivative dqdppn to B-DNA oligonucleotides."  Org. Biomol. Chem. 8, 648-654 (2010).
PubMed: 20090983

Assembly members:

Assembly members:
d(AGAGCTCT)2, polymer, 8 residues, Formula weight is not available
DQDPPN, non-polymer, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
d(AGAGCTCT)2: AGAGCTCT

Data sets:
Data typeCount
1H chemical shifts54

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1d(AGAGCTCT),11
2d(AGAGCTCT),21
3dqdppn,12
4dqdppn,22

Entities:

Entity 1, d(AGAGCTCT),1 8 residues - Formula weight is not available

1   DADGDADGDCDTDCDT

Entity 2, dqdppn,1 - . - Formula weight is not available

1   DQDPPN

Samples:

sample_1: d(AGAGCTCT)2 2 mM; dqdppn 4 mM; D2O 100%

sample_conditions_1: pH: 7; pressure: 1 atm; temperature: 328 K

Experiments:

NameSampleSample stateSample conditions
2D DQF-COSYsample_1isotropicsample_conditions_1
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H NOESYsample_1isotropicsample_conditions_1
2D 31P-1H COSYsample_1isotropicsample_conditions_1

Software:

FELIX, Accelrys Software Inc. - chemical shift assignment, processing

NMR spectrometers:

  • Bruker Avance 500 MHz
  • Bruker Avance 800 MHz