BMRB Entry 15667
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15667
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Citation: Bhunia, Anirban; Mohanram, Harini; Bhattacharjya, Surajit. "Lipopolysaccharide bound structures of the active fragments of fowlicidin-1, a
cathelicidin family of antimicrobial and antiendotoxic peptide from chicken,
determined by transferred nuclear overhauser effect spectroscopy" Biopolymers 92, 9-22 (2009).
PubMed: 18844294
Assembly members:
LK19, polymer, 19 residues, 2224.778 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: Solid phase peptide synthesis Host organism: solid phase peptide synthesis
Entity Sequences (FASTA):
LK19: LVIRTVIAGYNLYRAIKKK
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 124 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | LK19 | 1 |
Entities:
Entity 1, LK19 19 residues - 2224.778 Da.
| 1 | LEU | VAL | ILE | ARG | THR | VAL | ILE | ALA | GLY | TYR | ||||
| 2 | ASN | LEU | TYR | ARG | ALA | ILE | LYS | LYS | LYS |
Samples:
sample_1: LK19 0.5 mM; H2O 90%; D2O 10%
sample_conditions_1: pH: 4.5; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H trNOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
DYANA v1.5, Guntert, Mumenthaler and Wuthrich - refinement
NMR spectrometers:
- Bruker DRX 600 MHz