BMRB Entry 15544

Title:
Solution structure of designed peptide YW12D in the presence of SDS micelle
Deposition date:
2007-11-05
Original release date:
2008-08-19
Authors:
Bhunia, Anirban; Bhattacharjya, Surajit
Citation:

Citation: Bhunia, Anirban; Chua, Geok Lin; Domadia, Prerna; Warshakoon, Hemamali; Cromer, Jens; David, Sunil; Bhattacharjya, Surajit. "Interactions of a designed peptide with lipopolysaccharide: Bound conformation and anti-endotoxic activity"  Biochem. Biophys. Res. Commun. 369, 853-857 (2008).
PubMed: 18328260

Assembly members:

Assembly members:
YW12D_SDS, polymer, 12 residues, 1657.134 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: Standard F-moc solid phase peptide synthesised   Host organism: solid phase peptide synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
YW12D_SDS: YVKLWRMIKFIR

Data sets:
Data typeCount
1H chemical shifts84

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
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Assembly:

Entity Assembly IDEntity NameEntity ID
1YW12D_SDS1

Entities:

Entity 1, YW12D_SDS 12 residues - 1657.134 Da.

1   TYRVALLYSLEUTRPARGMETILELYSPHE
2   ILEARG

Samples:

sample_1: YW12D_SDS 0.5 mM

sample_conditions_1: pH: 4.5; temperature: 308 K

Experiments:

NameSampleSample stateSample conditions
2D 1H-1H TOCSYsample_1isotropicsample_conditions_1
2D 1H-1H trNOESYsample_1isotropicsample_conditions_1

Software:

DYANA v1.5, Guntert, Braun and Wuthrich - refinement

NMR spectrometers:

  • Bruker DRX 600 MHz