BMRB Entry 15413

Title:
High resolution NMR structure of YW12D in the presence of Lipopolysaccharide (LPS)
Deposition date:
2007-07-31
Original release date:
2008-08-18
Authors:
Bhattacharjya, S.; Bhunia, A.
Citation:

Citation: Bhunia, Anirban; Chua, Geok Lin; Domadia, Prerna; Warshakoon, Hemamali; Cromer, Jens; David, Sunil; Bhattacharjya, Surajit. "Interactions of a designed peptide with lipopolysaccharide:Bound conformation and anti-endotoxic activity"  Biochem. Biophys. Res. Commun. 369, 853-857 (2008).
PubMed: 18328260

Assembly members:

Assembly members:
YW12D, polymer, 12 residues, 1657.134 Da.

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
YW12D: YVKLWRMIKFIR

Data sets:
Data typeCount
1H chemical shifts86

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
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Assembly:

Entity Assembly IDEntity NameEntity ID
1YW12D1

Entities:

Entity 1, YW12D 12 residues - 1657.134 Da.

1   TYRVALLYSLEUTRPARGMETILELYSPHE
2   ILEARG

Samples:

sample_1: YW12D 0.6 mM; H2O 90%; D2O 10%

sample_conditions_1: pH: 4.8; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
TOCSY, transferred-NOESYsample_1isotropicsample_conditions_1

Software:

DYANA v1.5, Guntert, Braun and Wuthrich - refinement

NMR spectrometers:

  • Bruker DRX 600 MHz