BMRB Entry 15286
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15286
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Citation: Subramanian, Vivekanandan; D Jois, Seetharama; Kini, Manjunatha. "chemical shift values for Bungatoxin" .
Assembly members:
Bungatoxin, polymer, 65 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: 92438 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Bungarus Candidus
Experimental source: Production method: purified from the natural source Host organism: Bungarus Candidus snake venom
Entity Sequences (FASTA):
Bungatoxin: LTCLICPEKDCQKVHTCRNE
EKICVKRFYDKNQLGWRAQR
GCAVSCPKAKPNETVQCCST
DKCNK
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 395 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Bungatoxin | 1 |
Entities:
Entity 1, Bungatoxin 65 residues - Formula weight is not available
| 1 | LEU | THR | CYS | LEU | ILE | CYS | PRO | GLU | LYS | ASP | ||||
| 2 | CYS | GLN | LYS | VAL | HIS | THR | CYS | ARG | ASN | GLU | ||||
| 3 | GLU | LYS | ILE | CYS | VAL | LYS | ARG | PHE | TYR | ASP | ||||
| 4 | LYS | ASN | GLN | LEU | GLY | TRP | ARG | ALA | GLN | ARG | ||||
| 5 | GLY | CYS | ALA | VAL | SER | CYS | PRO | LYS | ALA | LYS | ||||
| 6 | PRO | ASN | GLU | THR | VAL | GLN | CYS | CYS | SER | THR | ||||
| 7 | ASP | LYS | CYS | ASN | LYS |
Samples:
sample_1: Bungatoxin from Bangarus Candidus 1 mM; H2O 90%; D2O 10%
sample_conditions_1: ionic strength: 0 M; pH: 5.5; pressure: 1 atm; temperature: 300 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
Software:
DYANA, Herrmann, Guntert and Wuthrich - structure solution
NMR spectrometers:
- Bruker Avance 800 MHz
- Bruker Avance 500 MHz