BMRB Entry 15130
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15130
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Citation: Venditti, Vincenzo; Bernini, Andrea; De Simone, Alfonso; Spiga, Ottavia; Prischi, Filippo; Niccolai, Neri. "MMD and NMR studies of alpha-bungarotoxin surface accessibility" Biochem. Biophys. Res. Commun. 356, 114-117 (2007).
PubMed: 17336923
Assembly members:
alpha-BTX, polymer, 74 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: obtained from a vendor
Entity Sequences (FASTA):
alpha-BTX: IVCHTTATSPISAVTCPPGE
NLCYRKMWCDAFCSSRGKVV
ELGCAATCPSKKPYEEVTCC
STDKCNPHPKQRPG
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 74 |
| 1H chemical shifts | 78 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | alpha-BTX | 1 |
Entities:
Entity 1, alpha-BTX 74 residues - Formula weight is not available
| 1 | ILE | VAL | CYS | HIS | THR | THR | ALA | THR | SER | PRO | ||||
| 2 | ILE | SER | ALA | VAL | THR | CYS | PRO | PRO | GLY | GLU | ||||
| 3 | ASN | LEU | CYS | TYR | ARG | LYS | MET | TRP | CYS | ASP | ||||
| 4 | ALA | PHE | CYS | SER | SER | ARG | GLY | LYS | VAL | VAL | ||||
| 5 | GLU | LEU | GLY | CYS | ALA | ALA | THR | CYS | PRO | SER | ||||
| 6 | LYS | LYS | PRO | TYR | GLU | GLU | VAL | THR | CYS | CYS | ||||
| 7 | SER | THR | ASP | LYS | CYS | ASN | PRO | HIS | PRO | LYS | ||||
| 8 | GLN | ARG | PRO | GLY |
Samples:
sample_1: alpha-BTX 1.0 mM
sample_conditions_1: pH: 6.0; pressure: 1 atm; temperature: 303 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-13C HSQC-TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
SPARKY, Goddard - chemical shift assignment
NMRPipe, Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax - processing
NMR spectrometers:
- Bruker Avance 600 MHz