BMRB Entry 5840

Title:
Chemical Shifts assignments for Frenatin 3 in both Triflouroethanol/water and water
Deposition date:
2003-06-22
Original release date:
2003-12-18
Authors:
Bowie, John; Llewellyn, Lyndon; Doyle, Jason; Wegener, Kate; Carver, John; Brinkworth, Craig
Citation:

Citation: Brinkworth, Craig; Carver, John; Wegener, Kate; Doyle, Jason; Llewellyn, Lyndon; Bowie, John. "The solution structure of frenatin 3, a neuronal nitric oxide synthase inhibitor from the giant tree frog, Litoria infrafrenata"  Biopolymers 70, 424-434 (2003).
PubMed: 14579314

Assembly members:

Assembly members:
Frenatin 3, polymer, 22 residues, 2179 Da.

Natural source:

Natural source:   Common Name: Giant Tree Frog   Taxonomy ID: 61195   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Litoria Infrafrenata

Experimental source:

Experimental source:   Production method: vendor

Entity Sequences (FASTA):

Entity Sequences (FASTA):
Frenatin 3: GLMSVLGHAVGNVLGGLFKP KS

Data sets:
Data typeCount
1H chemical shifts321
13C chemical shifts44

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1Frenatin 31

Entities:

Entity 1, Frenatin 3 22 residues - 2179 Da.

1   GLYLEUMETSERVALLEUGLYHISALAVAL
2   GLYASNVALLEUGLYGLYLEUPHELYSPRO
3   LYSSER

Samples:

Frenatin_3_in_TFE-water: Frenatin 3 4.1 mM; H2O 50%; Deuterated Trifluorethanol 50%

Frenatin_3_in_water: Frenatin 3 4.1 mM; H2O 100%

sample_cond_1: pH: 3.51; temperature: 298 K

sample_cond_2: pH: 3.05; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
NOESYnot availablenot availablenot available
QF-COSYnot availablenot availablenot available
TOCSYnot availablenot availablenot available
1Dnot availablenot availablenot available

Software:

No software information available

NMR spectrometers:

  • Varian INOVA 600 MHz

Related Database Links:

EMBL CAI77673
PRF 2208400C