BMRB Entry 53705
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR53705
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
All files associated with the entry
Citation: LEFRANC, Benjamin; COQUET, Laurent; DOUGHLA, Alexis; MEUDAL, Herve; RENWA, Theophile; NALPAS, Nicolas; GABANT, Guillaume; DUBESSY, Christophe; TUFFERY, Pierre; LOTH, Karine; CONLON, J Mickael; LEPRINCE, Jerome. "Characterization of Tryptolinophyllins from the Treefrog Boana boans Expands the Structural and Functional Diversity of the Trypytophyllin Family of Peptides" Sci. Rep. ., .-..
Assembly members:
entity_1, polymer, 7 residues, Formula weight is not available
Natural source: Common Name: Boana boans Taxonomy ID: 317327 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Boana boans
Experimental source: Production method: purified from the natural source
Entity Sequences (FASTA):
entity_1: XRPFPFL
| Data type | Count |
| 13C chemical shifts | 140 |
| 1H chemical shifts | 260 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Tryptolinophyllin | 1 |
Entities:
Entity 1, Tryptolinophyllin 7 residues - Formula weight is not available
| 1 | TPI | ARG | PRO | PHE | PRO | PHE | LEU |
Samples:
sample_1: Tryptolinophyllin-extracted 1.35 mM; Tryptolinophyllin-synth-NH2-A 1.35 mM; Tryptolinophyllin-synth-NH2-B 1.35 mM; Tryptolinophyllin-synth-OH-A 1.35 mM; Tryptolinophyllin-synth-OH-B 1.35 mM
sample_conditions_1: temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1D 1H | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-13C HSQC | sample_1 | isotropic | sample_conditions_1 |
Software:
CcpNMR - chemical shift assignment
TOPSPIN - collection
NMR spectrometers:
- Bruker AVANCE III HD 700 MHz