BMRB Entry 53328
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR53328
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Citation: Futagawa, Kei; Iijima, Mayumi; Zhang, Changyu; Nagata, Koji; Suzuki, Michio. "Conformational analysis of an SRCRD-derived peptide on hydroxyapatite surfaces using dispersive calcium phosphate particles
" Phys. Chem. Chem. Phys. 28, 20322-20335 (2026).
PubMed: 42573460
Assembly members:
entity_1, polymer, 20 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity_1: GDDYWDTNDGSGSGSDDVRG
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 94 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | SRCRDpep | 1 |
Entities:
Entity 1, SRCRDpep 20 residues - Formula weight is not available
| 1 | GLY | ASP | ASP | TYR | TRP | ASP | THR | ASN | ASP | GLY | |
| 2 | SER | GLY | SER | GLY | SER | ASP | ASP | VAL | ARG | GLY |
Samples:
sample_1: SRCRDpep 4 mM; hydroxyapatite 5 mg; D2O, [U-2H], 10%; DSS, [U-99% 2H], 1 mM; NaPi 20 mM
sample_conditions_1: ionic strength: 20 mM; pH: 6; pressure: 1 atm; temperature: 297 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1D 1H | sample_1 | isotropic | sample_conditions_1 |
Software:
CYANA - structure solution
NMRPipe - data analysis
SPARKY - peak picking
NMR spectrometers:
- JEOL ECA 600 MHz