BMRB Entry 52049
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR52049
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Citation: Rout, Saroj; Cadalbert, Riccardo; Schroeder, Nina; Wang, Julia; Zehnder, Johannes; Gampp, Olivia; Wiegand, Thomas; Guntert, Peter; Klingler, David; Kreutz, Christoph; Knoerlein, Anna; Hall, Jonathan; Greenwald, Jason; Riek, Roland. "An Analysis of Nucleotide-Amyloid Interactions Reveals Selective Binding to Codon-Sized RNA" J. Am. Chem. Soc. 145, 21915-21924 (2023).
PubMed: 37782045
Assembly members:
entity_1, polymer, 8 residues, Formula weight is not available
entity_2, polymer, 4 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 39 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | VAQAQINI | 1 |
| 2 | GUCA | 2 |
Entities:
Entity 1, VAQAQINI 8 residues - Formula weight is not available
| 1 | VAL | ALA | GLN | ALA | GLN | ILE | ASN | ILE |
Entity 2, GUCA 4 residues - Formula weight is not available
| 1 | G | U | C | A |
Samples:
sample_1: VAQAQINI, [U-100% 13C; U-100% 15N], 10 mg; GUCA, [U-10% 13C], 1.5 mg
sample_conditions_1: pH: 3; pressure: 1 atm; temperature: 283 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 13C-13C DARR | sample_1 | isotropic | sample_conditions_1 |
Software:
CYANA - chemical shift assignment, structure solution
NMR spectrometers:
- Bruker AVANCE III 850 MHz