BMRB Entry 6623
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6623
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Citation: Munte, Claudia; Vilela, Luciano; Kalbitzer, Hans; Garratt, Richard. "Solution Structure of Human Proinsulin C-Peptide" FEBS J. 272, 4284-4293 (2005).
PubMed: 16098208
Assembly members:
C-peptide, polymer, 31 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
C-peptide: EAEDLQVGQVELGGGPGAGS
LQPLALEGSLQ
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 602 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | C-peptide | 1 |
Entities:
Entity 1, C-peptide 31 residues - Formula weight is not available
| 1 | GLU | ALA | GLU | ASP | LEU | GLN | VAL | GLY | GLN | VAL | ||||
| 2 | GLU | LEU | GLY | GLY | GLY | PRO | GLY | ALA | GLY | SER | ||||
| 3 | LEU | GLN | PRO | LEU | ALA | LEU | GLU | GLY | SER | LEU | ||||
| 4 | GLN |
Samples:
sample_1: C-peptide 6 mM; D2O 5%; H2O 95%
sample_2: C-peptide 3 mM; TFE-d2 50%; H2O 50%
sample_3: C-peptide 1.2 mM; TFE-d2 80%; H2O 20%
conditions_1: pH: 7.0; temperature: 283 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| COSY | not available | not available | not available |
| TOCSY | not available | not available | not available |
| NOESY | not available | not available | not available |
Software:
No software information available
NMR spectrometers:
- Bruker DRX 600 MHz