BMRB Entry 5673

Click here to enlarge.

PDB ID: 1nau
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5673
MolProbity Validation Chart

NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry

Nicholas Rego and David Koes
3Dmol.js: molecular visualization with WebGL
Bioinformatics (2015) 31 (8): 1322-1324 doi:10.1093/bioinformatics/btu829

Select model:

I am color blind

Download raw data. Direct link to this display. Help

Title:

NMR Solution Structure of the Glucagon Antagonist [desHis1, desPhe6, Glu9]Glucagon Amide in the Presence of Perdeuterated Dodecylphosphocholine Micelles

Deposition date:

2003-01-23

Original release date:

2008-07-17

Authors:

Ying, J.; Ahn, J.-M.; Jacobsen, N.; Brown, M.; Hruby, V.

Citation:

Citation: Ying, J.; Ahn, J.-M.; Jacobsen, N.; Brown, M.; Hruby, V.. "NMR Solution Structure of the Glucagon Antagonist [desHis(1), desPhe(6), Glu(9)] Glucagon Amide in the Presence of Perdeuterated Dodecylphosphocholine Micelles" Biochemistry 42, 2825-2835 (2003).
PubMed: 12627948

Assembly members:

Assembly members:
Glucagon analogue, polymer, 28 residues, Formula weight is not available

Natural source:

Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapien

Experimental source:

Experimental source: Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
Glucagon analogue: SQGTTSEYSKYLDSRRAQDF VQWLMNTX

Data sets:

assigned_chemical_shifts
- chemical_shift_set_1

Data type	Count
1H chemical shifts	144

Additional metadata:

Assembly
Samples and Experiments
Software
Spectrometers
Hide all

Assembly:

Entity Assembly ID	Entity Name	Entity ID
1	Glucagon analogue	1

Entities:

Entity 1, Glucagon analogue 28 residues - Formula weight is not available

1

SER

GLN

GLY

THR

SER

GLU

TYR

SER

LYS

2

TYR

LEU

ASP

SER

ARG

ALA

GLN

ASP

PHE

3

VAL

GLN

TRP

LEU

MET

ASN

THR

NH2

Samples:

sample_1: Glucagon analogue 7 mM; sodium phosphate buffer 50 mM; dodecylphosphocholine-d38 283 mM; sodium azide 1 mM; H2O 90%; D2O 10%

sample_cond_1: ionic strength: 50 mM; pH: 6.0; pressure: 1 atm; temperature: 310 K

Experiments:

Name	Sample	Sample state	Sample conditions
DQF-COSY	sample_1	not available	sample_cond_1
2D TOCSY	sample_1	not available	sample_cond_1
2D NOESY	sample_1	not available	sample_cond_1

Software:

UXNMR - collection

FELIX v2000 - data analysis, processing

DGII vwithin InsightII 2000 - structure solution

DISCOVER vwithin InsightII 2000 - refinement

NMR spectrometers:

Bruker AMX 500 MHz