BMRB Entry 4298
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4298
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Citation: Vranken, Wim; Budesinsky, Milos; Martins, Jose; Fant, Franky; Boulez, Kris; Gras-Masse, Helene; Borremans, Frans. "Conformational Features of a Synthetic
Cyclic Peptide Corresponding to the
Complete V3 Loop of the RF HIV-1 Strain
in Water and Water/Trifluoroethanol
Solutions" Eur. J. Biochem. 236, 100-108 (1996).
Assembly members:
V3 loop, polymer, 35 residues, 3880.4 Da.
Natural source: Common Name: Human Immunodefiency Virus Taxonomy ID: 12721 Superkingdom: not available Kingdom: not available Genus/species: Lentivirus Human immunodeficiency virus
Experimental source: Production method: chemically synthesized
Entity Sequences (FASTA):
V3 loop: CTRPNNNTRKSITKGPGRVI
YATGQIIGDIRKAHC
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 255 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | V3_loop | 1 |
Entities:
Entity 1, V3_loop 35 residues - 3880.4 Da.
| 1 | CYS | THR | ARG | PRO | ASN | ASN | ASN | THR | ARG | LYS | ||||
| 2 | SER | ILE | THR | LYS | GLY | PRO | GLY | ARG | VAL | ILE | ||||
| 3 | TYR | ALA | THR | GLY | GLN | ILE | ILE | GLY | ASP | ILE | ||||
| 4 | ARG | LYS | ALA | HIS | CYS |
Samples:
sample_one: V3 loop 4.0 mM
sample_conditions_one: pH: 2.5; temperature: 275 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| magnitude COSY | sample_one | not available | not available |
| TOCSY | sample_one | not available | not available |
| NOESY | sample_one | not available | not available |
| CT-NOESY | sample_one | not available | not available |
Software:
UXNMR - Spectrum processing
PRONTO - Analysis of spectra
NMR spectrometers:
- Bruker AM-500 500 MHz