BMRB Entry 5439

Title:
pKa determinations for P4-Asp OMTKY3 (not salt added)
Deposition date:
2002-07-04
Original release date:
2003-03-20
Authors:
Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John
Citation:

Citation: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John. "NMR Determination of pKa Values for Asp, Glu, His, and Lys Mutants at Each Variable Contiguous Enzyme-inhibitor Contact Position of the Turkey Ovomucoid Third Domain"  Biochemistry 42, 2847-2856 (2003).
PubMed: 12627950

Assembly members:

Assembly members:
P4-Asp Turkey Ovomucoid Third Domain, polymer, 51 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: Turkey   Taxonomy ID: 9103   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Meleagris gallopavo

Experimental source:

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):

Entity Sequences (FASTA):
P4-Asp Turkey Ovomucoid Third Domain: VDCSEYPKPDCTLEYRPLCG SDNKTYGNKCNFCNAVVESN GTLTLSHFGKC

Data sets:
Data typeCount
pH NMR parameter values80
pKa values6

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1P4-Asp OMTKY31

Entities:

Entity 1, P4-Asp OMTKY3 51 residues - Formula weight is not available

1   VALASPCYSSERGLUTYRPROLYSPROASP
2   CYSTHRLEUGLUTYRARGPROLEUCYSGLY
3   SERASPASNLYSTHRTYRGLYASNLYSCYS
4   ASNPHECYSASNALAVALVALGLUSERASN
5   GLYTHRLEUTHRLEUSERHISPHEGLYLYS
6   CYS

Samples:

sample_1: P4-Asp Turkey Ovomucoid Third Domain 2 mM; KCl 0 mM; DSS 0.4 mM

conditions_set_1: ionic strength: 0 mM; pH: .; temperature: 298 K

Experiments:

NameSampleSample stateSample conditions
TOCSYnot availablenot availablenot available

Software:

No software information available

NMR spectrometers:

  • Bruker DMX 500 MHz

Related Database Links:

BMRB 1374 1375 4068 42 4864 4865 507 5411 5435 5438 5448 5518 5520
PDB
SWISS-PROT P05589 P52245 P68436